F16-LCMS-21097-MedChemExpress

File D:\DATA\A02\MONITOR\BIZ2016-720-WJ21-04461-LCMSA016.D Injection Date : 20 Jul 16 2:15 pm +0800 Tgt Mass(EZX) : 362.00 Sample Name : BIZ2016-720-WJ2 Location : P1-A-06 Acq. Operator : A02-Monitor Inj : 1 Spec. Reported : MS Integration Inj Volume : 3 ul Acq. Method : D:\METHODS\1-POS-MON.M Analysis Method : D:\METHODS\1-POS-MON.M Catalog No : HY-100395 Batch#21097 Easy-Access Method: '1-POS-MON' 362.00 Method Info : Mobile Phase: A: water(0.01%TFA) B : ACN Gradient: 5%B increase to 95%B within1.5min, 95%B for 1.5min,back to 5%B within 0.01min. Flow Rate: 2.0 mL/min Column: Sunfire C18 4.6*50mm 3.5um Oven Temperature: 50 C Mass Range:103-1500min*00.5

1 1.5

2 2.53mV

23.22

23.2225

*ADC1 A, ELSD

min*00.5

1 1.5

2 2.53mAU

1000

*DAD1 A, Sig=214,4 Ref=off

1.177min*

00.51

1.52

2.53mAU

500

*DAD1 B, Sig=254,4 Ref=off

1.177min 00.51 1.5

2 2.530

200000

400000

MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70

1.178

2.805min 00.5

1 1.5

2 2.530

100

200

Ion 363, MSD1 363,Target Mass 362 +H Positive, EIC=362.7:363.7

Integration Results for ADC1 A, ELSD RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------|

Integration Results for DAD1 A, Sig=214,4 Ref=off

RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------| 1.18 0.01 1503.77 2205.76 100.00

Integration Results for DAD1 B, Sig=254,4 Ref=off

RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------| 1.18 0.01 861.94 1274.17 100.00

Ret. Time: 1.18 <<<< POSITIVE SPECTRA >>>>m/z 200400600800100012000

20000

40000

60000

80000

100000

120000

140000

ES-API Positive

236.1 235.2Ret. Time: 2.81

m/z 2004006008001000120014000

2000

4000

6000

8000

10000

12000

14000

ES-API Positive

675.5 219.0 193.9 235.1 159.0 339.3 361.3 338.3 360.3