=====================================================================Acq. Operator : Yang Qian(LCMS-02) Seq. Line : 80
Acq. Instrument : HY-LCMS-02 Location : P2-D-01Injection Date : 12/7/2015 4:46:04 PM Inj : 1
Inj Volume : 3.000 μl
Acq. Method : D:\AGLIENT 1260\DATA\20151207\20151207 2015-12-07 10-06-12\100-1000MS+3MIN- 1.5_(0.02%FA)-BD.M
Last changed : 12/7/2015 10:06:12 AM by Yang Qian(LCMS-02)
Analysis Method : D:\AGLIENT 1260\DATA\20151207\20151207 2015-12-07 10-06-12\100-1000MS+7MIN_ 1.5(0.02%FA)-BD.M (Sequence Method)
Last changed : 12/8/2015 1:13:04 PM by Yang Qian(LCMS-02) (modified after loading)
Method Info : Postive,MS:100-1000,Column ID:A-RP-85,50℃
Catalog No : HY-N0421 Batch#18850 A-RP-134
Additional Info : Peak(s) manually integrated
min
0.51 1.52 2.53mAU
100200300 DAD1 B, Sig=214,4 Ref=off (D:\AGLIENT...60\DATA\20151207\20151207 2015-12-07 10-06-12\BIZ2015-D07-WJ11.D)
1.855 1.943
2.016
2.075
2.215
2.479
===================================================================== Area Percent Report =====================================================================
Sorted By : Signal Multiplier : 1.0000Dilution : 1.0000
Do not use Multiplier & Dilution Factor with ISTDs
Signal 1: DAD1 B, Sig=214,4 Ref=off
Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %
----|-------|----|-------|----------|----------|--------| 1 1.855 MM 0.0374 1.57575 7.01865e-1 0.1348 2 1.943 MM 0.0432 2.42575 9.36471e-1 0.2076 3 2.016 MF 0.0348 11.49845 5.50038 0.9839 4 2.075 FM 0.0436 1146.42224 438.19327 98.0977 5 2.215 MM 0.0398 2.54767 1.06718 0.2180 6 2.479 MM 0.0419 4.18332 1.66594 0.3580
Totals : 1168.65319 448.06510
===================================================================== *** End of Report ***
=====================================================================Acq. Operator : Yang Qian(LCMS-02) Seq. Line : 80
Acq. Instrument : HY-LCMS-02 Location : P2-D-01Injection Date : 12/7/2015 4:46:04 PM Inj : 1
Inj Volume : 3.000 μl
Acq. Method : D:\AGLIENT 1260\DATA\20151207\20151207 2015-12-07 10-06-12\100-1000MS+3MIN- 1.5_(0.02%FA)-BD.M
Last changed : 12/7/2015 10:06:12 AM by Yang Qian(LCMS-02)
Analysis Method : D:\AGLIENT 1260\DATA\20151207\20151207 2015-12-07 10-06-12\100-1000MS+7MIN_ 1.5(0.02%FA)-BD.M (Sequence Method)
Last changed : 12/8/2015 10:42:46 AM by Yang Qian(LCMS-02) (modified after loading)
Method Info : Postive,MS:100-1000,Column ID:A-RP-85,50℃
Catalog No : HY-N0421 Batch#18850 A-RP-134
Additional Info : Peak(s) manually integrated
min
0.51 1.52 2.5350000
100000150000200000 MSD1 TIC, MS File (D:\AGLIENT 1260\DATA\20151207\20151207 2015-12-07 10-06-12\BIZ2015-D07-WJ11.D) ES-API, Pos, Sca
2.080
MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts.
Reportable Ion Abundance: > 10%.
Retention Mol. Weight Time (MS) MS Area or Ion
2.080 902491 444.30 I 44
3.30 I
m/z
100
200
300
400
500
600
700
800
900
20406080100*MSD1 SPC, time=2.053:2.108 of D:\AGLIENT 1260\DATA\20151207\20151207 2015-12-07 10-06-12\BIZ2015-D07-WJ11.D ES-API,Max: 119888
445.3
444.3 443.3
*** End of Report ***