File D:\DATA\A02\MONITOR\BIZ2016-720-WJ21-04461-LCMSA016.D Injection Date : 20 Jul 16 2:15 pm +0800 Tgt Mass(EZX) : 362.00 Sample Name : BIZ2016-720-WJ2 Location : P1-A-06 Acq. Operator : A02-Monitor Inj : 1 Spec. Reported : MS Integration Inj Volume : 3 ul Acq. Method : D:\METHODS\1-POS-MON.M Analysis Method : D:\METHODS\1-POS-MON.M Catalog No : HY-100395 Batch#21097 Easy-Access Method: '1-POS-MON' 362.00 Method Info : Mobile Phase: A: water(0.01%TFA) B : ACN Gradient: 5%B increase to 95%B within1.5min, 95%B for 1.5min,back to 5%B within 0.01min. Flow Rate: 2.0 mL/min Column: Sunfire C18 4.6*50mm 3.5um Oven Temperature: 50 C Mass Range:103-1500min*00.5
1 1.5
2 2.53mV
23.22
23.2225
*ADC1 A, ELSD
min*00.5
1 1.5
2 2.53mAU
1000
*DAD1 A, Sig=214,4 Ref=off
1.177min*
00.51
1.52
2.53mAU
500
*DAD1 B, Sig=254,4 Ref=off
1.177min 00.51 1.5
2 2.530
200000
400000
MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70
1.178
2.805min 00.5
1 1.5
2 2.530
100
200
Ion 363, MSD1 363,Target Mass 362 +H Positive, EIC=362.7:363.7
Integration Results for ADC1 A, ELSD RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------|
Integration Results for DAD1 A, Sig=214,4 Ref=off
RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------| 1.18 0.01 1503.77 2205.76 100.00
Integration Results for DAD1 B, Sig=254,4 Ref=off
RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------| 1.18 0.01 861.94 1274.17 100.00
Ret. Time: 1.18 <<<< POSITIVE SPECTRA >>>>m/z 200400600800100012000
20000
40000
60000
80000
100000
120000
140000
ES-API Positive
236.1 235.2Ret. Time: 2.81
m/z 2004006008001000120014000
2000
4000
6000
8000
10000
12000
14000
ES-API Positive
675.5 219.0 193.9 235.1 159.0 339.3 361.3 338.3 360.3